Module also offered within study programmes:
General information:
Name:
Atomic Force Microscopy and its variants in advanced measurements
Course of study:
2019/2020
Code:
CTCH-2-324-s
Faculty of:
Materials Science and Ceramics
Study level:
Second-cycle studies
Specialty:
-
Field of study:
Chemical Technology
Semester:
3
Profile of education:
Academic (A)
Lecture language:
Polish
Form and type of study:
Full-time studies
Course homepage:
 
Responsible teacher:
dr Niemiec Wiktor (wniemiec@agh.edu.pl)
Module summary

The module presents the Atomic Force Microscopy and a number of selected derivative microscopies and their use in various fields of science.

Description of learning outcomes for module
MLO code Student after module completion has the knowledge/ knows how to/is able to Connections with FLO Method of learning outcomes verification (form of completion)
Social competence: is able to
M_K001 Student is able to formulate a question based on scientific presentation, for which answers can give better insight into discussed topic. TCH2A_K02 Activity during classes
Skills: he can
M_U001 Student is able to find scientific articles on selected topic and on their basis prepare a presentation in english about the results of various scientific experiments. TCH2A_U06 Presentation
Knowledge: he knows and understands
M_W001 Student has knowledge about the principles of operation, advantages and restrictions of various microscopies based on Atomic Force Microscopy. TCH2A_W02, TCH2A_W03 Presentation
M_W002 Student has knowledge about the use and usefulness of different microscopies based on Atomic Force Microscopy in different fields of science. Student has knowledge which materials and materials' properties can be investigated with these miscroscopies, as well as how to modify the experiments to acquire additional information about sample properties.. TCH2A_W02, TCH2A_W03, TCH2A_W06 Presentation,
Activity during classes
Number of hours for each form of classes:
Sum (hours)
Lecture
Audit. classes
Lab. classes
Project classes
Conv. seminar
Seminar classes
Pract. classes
Zaj. terenowe
Zaj. warsztatowe
Prace kontr. przejść.
Lektorat
30 0 0 0 0 0 30 0 0 0 0 0
FLO matrix in relation to forms of classes
MLO code Student after module completion has the knowledge/ knows how to/is able to Form of classes
Lecture
Audit. classes
Lab. classes
Project classes
Conv. seminar
Seminar classes
Pract. classes
Zaj. terenowe
Zaj. warsztatowe
Prace kontr. przejść.
Lektorat
Social competence
M_K001 Student is able to formulate a question based on scientific presentation, for which answers can give better insight into discussed topic. - - - - - + - - - - -
Skills
M_U001 Student is able to find scientific articles on selected topic and on their basis prepare a presentation in english about the results of various scientific experiments. - - - - - + - - - - -
Knowledge
M_W001 Student has knowledge about the principles of operation, advantages and restrictions of various microscopies based on Atomic Force Microscopy. - - - - - + - - - - -
M_W002 Student has knowledge about the use and usefulness of different microscopies based on Atomic Force Microscopy in different fields of science. Student has knowledge which materials and materials' properties can be investigated with these miscroscopies, as well as how to modify the experiments to acquire additional information about sample properties.. - - - - - + - - - - -
Student workload (ECTS credits balance)
Student activity form Student workload
Summary student workload 75 h
Module ECTS credits 3 ECTS
Udział w zajęciach dydaktycznych/praktyka 30 h
przygotowanie projektu, prezentacji, pracy pisemnej, sprawozdania 20 h
Realization of independently performed tasks 25 h
Module content
Seminar classes (30h):

The classes are divided into two parts. The first part consist of a series of lectures about:
- history of microscopy, optical and electron microscopies as basic methods of surface morphology investigation;
- Atomic Force Microscopy, the physics behind the measurements, schematic construction of microscope, working modes, sample properties measured, error sources, sample usage;
- selected derivative microscopies like Electrostatic Force Microscopy, Kelvin Probe Force Microscopy and Tip Enhanced Raman Spectroscopy, the physics behind the measurements, schematic construction of microscopes and their usefulness in different fields of science.
The second part consists of students’ presentations about different researches in which Atomic Force Microscopy played a vital role. Students are able to choose articles from any field of science (the one that interests them is recommended).

Additional information
Teaching methods and techniques:
  • Seminar classes: Na zajęciach seminaryjnych podstawą jest prezentacja multimedialna oraz ustna prowadzona przez studentów. Kolejnym ważnym elementem kształcenia są odpowiedzi na powstałe pytania, a także dyskusja studentów nad prezentowanymi treściami.
Warunki i sposób zaliczenia poszczególnych form zajęć, w tym zasady zaliczeń poprawkowych, a także warunki dopuszczenia do egzaminu:

Participation rules in classes:
  • Seminar classes:
    – Attendance is mandatory: Yes
    – Participation rules in classes: Studenci prezentują na forum grupy temat wskazany przez prowadzącego oraz uczestniczą w dyskusji nad tym tematem. Ocenie podlega zarówno wartość merytoryczna prezentacji, jak i tzw. kompetencje miękkie.
Method of calculating the final grade:

Students can earn between 3.0 to 5.0 points for presentation. Additional points can be acquired by:
- answering questions regarding presentation given by the student (0.0-0.2 per answer);
- asking relevant questions after another student’s presentation (0.1-0.3 per question);
- being present on every seminar (0.3);
- preparing the presentation for first two seminars with students’ presentation (varies).
The points are converted to the closest mark (i.e. 3.0-3.2 points to 3.0, 3.3-3.7 to 3.5, 3.8-4.2 to 4.0, 4.3-4.7 to 4.5 and 4.8+ to 5.0).

Sposób i tryb wyrównywania zaległości powstałych wskutek nieobecności studenta na zajęciach:

Prerequisites and additional requirements:

None.

Recommended literature and teaching resources:

Review articles about the use of Atomic Force Microscopy methods in different fields of science (the exact articles can vary depending on student’s scientific interests).

Scientific publications of module course instructors related to the topic of the module:

Handke, B., Klita, Ł., Niemiec, W., Self-assembly of dodecaphenyl POSS thin films (2017) Surface Science, 666, pp. 70-75. DOI: 10.1016/j.susc.2017.08.023
Klimek, K., Przekora, A., Benko, A., Niemiec, W., Blazewicz, M., Ginalska, G., The use of calcium ions instead of heat treatment for β-1,3-glucan gelation improves biocompatibility of the β-1,3-glucan/HA bone scaffold (2017) Carbohydrate Polymers, 164, pp. 170-178. DOI: 10.1016/j.carbpol.2017.02.015
Wesełucha-Birczyńska, A., Stodolak-Zych, E., Turrell, S., Cios, F., Krzuś, M., Długoń, E., Benko, A., Niemiec, W., Błazewicz, M., Vibrational spectroscopic analysis of a metal/carbon nanotube coating interface and the effect of its interaction with albumin (2016) Vibrational Spectroscopy, 85, pp. 185-195. DOI: 10.1016/j.vibspec.2016.04.008
Długoń, E., Szymańska, M., Leśniak, M., Jeleń, P., Niemiec, W., Sitarz, M., Investigation on bioactivity of zirconium-calcium coatings on titanium surface obtained by sol-gel and electrophoretic deposition (EPD) methods (2016) Key Engineering Materials, 687, pp. 65-70. DOI: 10.4028/www.scientific.net/KEM.687.65
Wytrwal, M., Koczurkiewicz, P., Zrubek, K., Niemiec, W., Michalik, M., Kozik, B., Szneler, E., Bernasik, A., Madeja, Z., Nowakowska, M., Kepczynski, M., Growth and motility of human skin fibroblasts on multilayer strong polyelectrolyte films (2016) Journal of Colloid and Interface Science, 461, pp. 305-316. DOI: 10.1016/j.jcis.2015.09.039
Dlugon, E., Simka, W., Fraczek-Szczypta, A., Niemiec, W., Markowski, J., Szymanska, M., Blazewicz, M., Carbon nanotube-based coatings on titanium (2015) Bulletin of Materials Science, 38 (5), pp. 1339-1344. DOI: 10.1007/s12034-015-1019-4
Długoń, E., Niemiec, W., Fra̧czek-Szczypta, A., Jeleń, P., Sitarz, M., Błazewicz, M., Spectroscopic studies of electrophoretically deposited hybrid HAp/CNT coatings on titanium (2014) Spectrochimica Acta – Part A: Molecular and Biomolecular Spectroscopy, 133, pp. 872-875. DOI: 10.1016/j.saa.2014.06.064
Kopeć, M., Niemiec, W., Laschewsky, A., Nowakowska, M., Zapotoczny, S., Photoinduced energy and electron transfer in micellar multilayer films (2014) Journal of Physical Chemistry C, 118 (4), pp. 2215-2221. DOI: 10.1021/jp410808z
Plewa, A., Niemiec, W., Filipowska, J., Osyczka, A.M., Lach, R., Szczubiałka, K., Nowakowska, M., Photocrosslinkable diazoresin/pectin films – Synthesis and application as cell culture supports (2011) European Polymer Journal, 47 (8), pp. 1503-1513. DOI: 10.1016/j.eurpolymj.2011.06.002
Wybrańska, K., Niemiec, W., Szczubiałka, K., Nowakowska, M., Morishima, Y., Adenine molecularly imprinted polymer-coated submicrometer silica gel particles (2010) Chemistry of Materials, 22 (18), pp. 5392-5399. DOI: 10.1021/cm100845u
Niemiec, W., Zapotoczny, S., Szczubiałka, K., Laschewsky, A., Nowakowska, M., Nanoheterogeneous multilayer films with perfluorinated domains fabricated using the layer-by-layer method (2010) Langmuir, 26 (14), pp. 11915-11920. DOI: 10.1021/la1012044

Additional information:

None